HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dinitrosalicylaldehyde → 3-(4-methoxybenzylsulfonyl)-6,8-dinitro-2H-chromen-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dinitrosalicylaldehyde | HCID 75571 | — |
| Reactant | 4-Methoxybenzyl-sulfonylacetic acid | HCID 12097414 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 3-(4-methoxybenzylsulfonyl)-6,8-dinitro-2H-chromen-2-one | HCID 11510003 | — |
Reaction Steps
A solution of 3,5-dinitrosalicylaldehyde (1 mmol) and 2-(4-methoxybenzylsulfonyl)acetic acid (1 mmol) in acetic acid (10 mL) was subjected to the General Procedure 2, Method A to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143428B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-3ca18664020f4cbd9d959949398069d5 |
| Source note | uspto-grants-2012_03 |