HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 54033049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | HCID 20556023 | HCID 20556023 | — |
| Reactant | 4-Methylocta-4-ene-1,7-diyne-3-ol | HCID 54236197 | — |
| Product | HCID 54033049 | HCID 54033049 | 87.5% |
Reaction Steps
By the same procedure as in Example 1, 1.22 g (10.0 millimoles) of 4-methylocta-4-ene-1,7-diyne-3-ol, 2.66 g (10.0 millimoles) of α-isopropyl-3,4-dichlorophenylacetyl chloride and 1.58 g (20.0 millimoles) of pyridine are reacted, followed by purification on silica gel column. Thus, 3.18 g of the objective ester is obtained as a pale yellow oily substance (87.5% of theoretical yield). nD24.0 1.5314.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04309439 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-c9522bce0680450baac7821fc204df27 |
| Source note | uspto-grants-1982_01 |