HCID 54080367, compound → HCID 54395225, compound

HRID 1105632Notes

Reaction equation

C([NH:3][C:4]([CH3:22])([CH3:21])[CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][C:10]([C:13]([CH3:20])=[CH:14][C:15]([O:17][CH2:18]C)=[O:16])=[CH:9][CH:8]=1)=O.[2H]C(Cl)(Cl)Cl.[2H]O[2H]>>[C:15]([CH:14]=[C:13]([C:10]1[CH:9]=[CH:8][C:7]([CH2:6][CH2:5][C:4]([CH3:22])([CH3:21])[NH2:3])=[CH:12][CH:11]=1)[CH3:20])([O:17][CH3:18])=[O:16]

Participants

Reactant 2

HCID 54080367HCID 54080367, compound

HCID 86585196CDCl3 D2O

Product 1

HCID 54395225HCID 54395225, compound

Procedure

This was prepared in an identical manner to the compound described in Description 6 using N-formyl-3-{4-(2-carboethoxy-1-methylethenyl)phenyl}-1, 1-dimethylpropanamine. τ(CDCl3 /D2O(8.8 (6H, s) 8.5-8.1 (2H, m), 7.48 (3H, d, J=1.5 Hz), 7.5-7.1 (2H, m), 6.3 (3H, s), {4.1 (broad) +3.88 (q, J=1.5 Hz), Total 1H}, 2.8 (2H, d, J=7 Hz), 2.55 (2H, d, J=7 Hz).

Workup

customThis was prepared in an identical manner to the compound

Sources & evidence

ORD record: ord-4e51aecc183040a88898de9526eb3436
Source dataset: uspto-grants-1982_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04309443

Reaction notes

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