Methyl 2-bromopropionate → HCID 15587057, compound

HRID 1105742Notes

Reaction equation

HRID 1105742 reaction equation
[CH3:1][N:2]([C:14]1[CH:19]=[CH:18][C:17]([OH:20])=[CH:16][CH:15]=1)[C:3]1[N:4]=[N:5][C:6]2[CH:12]=[C:11]([Cl:13])[CH:10]=[CH:9][C:7]=2[N:8]=1.Br[CH:22]([CH3:27])[C:23]([O:25][CH3:26])=[O:24]>>[CH3:1][N:2]([C:14]1[CH:19]=[CH:18][C:17]([O:20][CH:22]([CH3:27])[C:23]([O:25][CH3:26])=[O:24])=[CH:16][CH:15]=1)[C:3]1[N:4]=[N:5][C:6]2[CH:12]=[C:11]([Cl:13])[CH:10]=[CH:9][C:7]=2[N:8]=1

Participants

3

Reactant 2

HCID 95576Methyl 2-bromopropionateHCID 15587055HCID 15587055, compound

Product 1

HCID 15587057HCID 15587057, compound

Procedure

4-[N-Methyl-N-(7-chloro-1,2,4-benzotriazin-3-yl)-amino]phenol was reacted with methyl 2-bromopropionate following essentially the same procedure as that described in Example 1 part (b) to give the title compound, mp 120° C.

Sources & evidence

ORD record
ord-0e4f895c16e2428d8e9a3ac144abfffe
Source dataset
uspto-grants-1982_01
Patent number
US04310347

Reaction notes

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