Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Caprolactam | HCID 7768 | — |
| Reactant | Vinyl isocyanate | HCID 77094 | — |
| Reactant | Isocyanate | HCID 105034 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Vinyl isocyanate caprolactam | HCID 86738431 | — |
Reaction Steps
113 parts of ε-caprolactam and 91 parts of ethyl acetate (+0.015% of dibutyl-tin dilaurate) are introduced into a reaction vessel and heated to about 50° C. A mixture of 69 parts of vinyl isocyanate and 91 parts of ethyl acetate is then added dropwise in the course of 1 hour. The reaction is then allowed to continue for 5 hours. A light yellow clear solution is obtained. Blocked isocyanate content: 11.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04310398 |
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| Source dataset | uspto-grants-1982_01 |
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| ORD ID | ord-b8c0f43964014c6ea05750e18deee085 |
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| Source note | uspto-grants-1982_01 |
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