HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 20555085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 20555092 | HCID 20555092 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20555085 | HCID 20555085 | — |
Reaction Steps
10.0 g of 2-allyloxy-3-nitrophenol, 27 g of potassium carbonate and 54 ml of epichlorohydrin in 300 ml of acetone are stirred under reflux for 15-20 hours. After filtering the reaction mixture and evaporating the filtrate, crude 2-allyloxy-1-(2,3-epoxy-propoxy)-3-nitrobenzene is obtained and this can be used further as such.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04310527 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-1308cdf72f24459a9e9c7f347d481b8f |
| Source note | uspto-grants-1982_01 |