HCID 12901528, compound → HCID 12901515, compound

HRID 1105826Notes

Reaction equation

HRID 1105826 reaction equation
[CH2:1]([O:4][C:5]1[C:13]2[N:12](C)[C:11](=O)[NH:10][C:9]=2[CH:8]=[CH:7][CH:6]=1)[CH:2]=[CH2:3]>C1(C)C=CC=CC=1>[CH2:1]([O:4][C:5]1[CH:6]=[CH:7][CH:8]=[C:9]([NH2:10])[C:13]=1[NH:12][CH3:11])[CH:2]=[CH2:3]

Participants

3

Reactant 1

HCID 12901528HCID 12901528, compound

Product 1

HCID 12901515HCID 12901515, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

4-Allyloxy-3-methyl-benzimidazol-2-one, which has a melting point of 167°-168°, is obtained analogously to Example 10c) from 5.4 g of 1-allyloxy-2-methylamino-3-aminobenzene and 6.1 g N,N'-carbonyldiimidazole in 100 ml of toluene, after working up and subsequently recrystallising from toluene.

Sources & evidence

ORD record
ord-4bfb7b32d317462f8dc88eb478a3f275
Source dataset
uspto-grants-1982_01
Patent number
US04310527

Reaction notes

Loading…