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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1106067Generated: October 27, 2026

Thionyl Chloride → 3-(Acetylthio)-2-(methylthio)propionic acid chloride

https://huagongshe.com/reaction/1106067

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
Reactant3-(Acetylthio)-2-(methylthio)propionic acidHCID 20539692—
Product3-(Acetylthio)-2-(methylthio)propionic acid chlorideHCID 54341183—

Reaction Steps

The 3-(acetylthio)-2-(methylthio)propionic acid is refluxed in thionyl chloride for two hours. The reaction mixture is distilled to remove excess thionyl chloride and the product is distilled in vacuo to yield 3-(acetylthio)-2-(methylthio)propionic acid chloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04311697
Source datasetuspto-grants-1982_01
ORD IDord-417e0a7bcd5240969eb7fc2fc6b45f4d
Source noteuspto-grants-1982_01