Ammonia → HCID 57014803, compound

HRID 1106076Notes

Reaction equation

HRID 1106076 reaction equation
C([S:4][CH2:5][C:6]([N:8]1[C@H:18]([C:19]([OH:21])=[O:20])[CH2:17][C:10]2([C:14](=[O:15])[CH2:13][CH2:12][C:11]2=[O:16])[CH2:9]1)=[O:7])(=O)C.N>>[SH:4][CH2:5][C:6]([N:8]1[C@H:18]([C:19]([OH:21])=[O:20])[CH2:17][C:10]2([C:14](=[O:15])[CH2:13][CH2:12][C:11]2=[O:16])[CH2:9]1)=[O:7]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 57267278HCID 57267278, compound

Product 1

HCID 57014803HCID 57014803, compound

Procedure

The product from part (a) is hydrolyzed with concentrated ammonia according to the procedure of Example 2 to yield (8S)-7-(2-mercapto-1-oxoethyl)-1,4-dioxo-7-azaspiro[4.4]nonane-8-carboxylic acid.

Sources & evidence

ORD record
ord-94ae35b271bb44eca9e67addaada3bf2
Source dataset
uspto-grants-1982_01
Patent number
US04311697

Reaction notes

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