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HRID1106100

反应详情

EQUATION

反应方程式

HRID 1106100 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)O
HCID176

Acetic Acid

C2H4O2

结构：COc1ccc(C=O)cc1O
HCID12127

3-Hydroxy-4-methoxy-benzaldehyde

C8H8O3

结构：CC1=NN(c2ccc(C(=O)O)cc2)C(=O)C1
HCID109029

4-(3-Methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)benzoic acid

C11H10N2O3

PRODUCTS

生成物

1
结构：COc1cccc(C=C2C(=O)N(c3ccc(C(=O)O)cc3)N=C2C)c1O
HCID1226948

未命名化合物

PROCEDURE

实验过程

218 g (1 mole) of 1-p-carboxyphenyl-3-methyl-2-pyrazolin-5-one and 152 g (1 mole) of iso-vanillin were suspended in 1000 ml of acetic acid and refluxed for 3 h. After cooling down to room temperature the dye was filtered with suction and rinsed with acetone.

WORKUP

后处理

  1. temperaturerefluxed for 3 h
  2. filtrationwas filtered with suction
  3. washrinsed with acetone