HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → HCID 136203571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | 1-Phenyl-3-carboxy-5-pyrazolone | HCID 67061 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 136203571 | HCID 136203571 | — |
Reaction Steps
204 g (1 mole) of 1-phenyl-3-carboxy-2-pyrazolin-5-one and 122 g (1 mole) of p-hydroxybenzaldehyde were dissolved in 1000 ml of methanol. After a few minutes of refluxing the dye started crystallizing and after 1 h of boiling the reaction mixture was cooled to room temperature. The dye was filtered with suction and rinsed with methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04311787 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-9cbfd77500d348baba10109dab3ba9ed |
| Source note | uspto-grants-1982_01 |