HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53981280, compound → HCID 20482537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53981280 | HCID 53981280 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20482537 | HCID 20482537 | — |
Reaction Steps
A solution of 4 g. 2-(ethoxycarbonyl)vinyl 4-(16-bromohexadecylamino)benzoate and 400 mg. 10% palladium-on-carbon in 100 ml. tetrahydrofuran is hydrogenated at 50 psi until hydrogen uptake stops. The catalyst is filtered, the solution is evaporated, and the residue is crystallized from acetonitrile to yield 2-(ethoxycarbonyl)ethyl 4-(16-bromohexadecylamino)benzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04311846 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-ed8d39a17a8a4cc5a2b81b88d9f0064c |
| Source note | uspto-grants-1982_01 |