HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 20482535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | HCID 20482503 | HCID 20482503 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 20482535 | HCID 20482535 | — |
Reaction Steps
Anhydrous hydrogen bromide is passed rapidly into a solution of 5 g. of 4-(10-undecenylamino)benzoic acid and 1 g. of dibenzoyl peroxide in 300 ml. of 1,2-dimethoxyethane for 1 hour. Partial evaporation of the solvent affords a crystalline solid which is separated by filtration and recrystallized from ether-petroleum ether to yield the product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04311846 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-e04d36896bef4f728ffb73ceba0bcab2 |
| Source note | uspto-grants-1982_01 |