HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylpyridine → Ethyl 2-(2-Butyl)-3-hydroxy-3-methyl-3-(3-pyridyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | Ethyl 3-methylpentanoate | HCID 560255 | — |
| Product | Ethyl 2-(2-Butyl)-3-hydroxy-3-methyl-3-(3-pyridyl)propionate | HCID 54531343 | — |
Reaction Steps
Analysis of the pyrolysis product mixture by gas chromatography and preparative thin layer chromatography indicates that the mixture consists of 12 milligrams of the hydroxy ester starting material, and 85 milligrams of a 1:1 mixture of 3-acetylpyridine and ethyl β-methylvalerate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04312368 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-9856087d169d4c7f9a4c2cd044160d48 |
| Source note | uspto-grants-1982_01 |