HuagongsheHuagongshe Chemistry Print Report · For research reference only
Amyl Acetate → Amyl 3-Hydroxy-3-methyl-3-(4-pyridyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Amyl Acetate | HCID 12348 | — |
| Reactant | 4-Acetylpyridine | HCID 14282 | — |
| Product | Amyl 3-Hydroxy-3-methyl-3-(4-pyridyl)propionate | HCID 20441861 | — |
Reaction Steps
A 100 milligram quantity of the hydroxy ester described in Example III is pyrolyzed in a sealed tube at 400° C. for 3 minutes. Analysis of the pyrolysis mixture by gas chromatography indicates the presence of about 30% of a mixture in a 1:1 ratio of amyl acetate and 4-acetylpyridine. The remainder of the mixture contains unreacted starting material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04312368 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-f9b23d518ce24be28e1dde3284ee6ee2 |
| Source note | uspto-grants-1982_01 |