Citric Acid → HCID 131712652, compound

HRID 1106199Notes

Reaction equation

HRID 1106199 reaction equation
[CH2:1](Br)[CH:2]=[CH2:3].[OH-].[C:6]([OH:18])(=[O:17])[CH2:7][C:8]([CH2:13][C:14]([OH:16])=[O:15])([C:10]([OH:12])=[O:11])[OH:9].[N:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[C:6]([O-:18])(=[O:17])[CH2:7][C:8]([CH2:13][C:14]([O-:16])=[O:15])([C:10]([O-:12])=[O:11])[OH:9].[CH2:1]([N+:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH:2]=[CH2:3].[CH2:1]([N+:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH:2]=[CH2:3].[CH2:1]([N+:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH:2]=[CH2:3]

Participants

5

Procedure

Pyridine is reacted with allyl bromide; the halide intermediate is converted to the hydroxide with Rexyn 201, and then reacted with citric acid.

Sources & evidence

ORD record
ord-17f89c08f8e544899c67a85bfcc8705f
Source dataset
uspto-grants-1982_01
Patent number
US04312367

Reaction notes

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