Citric Acid → HCID 131712653, compound

HRID 1106200Notes

Reaction equation

HRID 1106200 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH3:7])[C:2]=1[CH3:8].CI.[OH-].[C:12]([OH:24])(=[O:23])[CH2:13][C:14]([CH2:19][C:20]([OH:22])=[O:21])([C:16]([OH:18])=[O:17])[OH:15]>>[C:12]([O-:24])(=[O:23])[CH2:13][C:14]([CH2:19][C:20]([O-:22])=[O:21])([C:16]([O-:18])=[O:17])[OH:15].[CH3:12][N+:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH3:7])[C:2]=1[CH3:8].[CH3:12][N+:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH3:7])[C:2]=1[CH3:8].[CH3:12][N+:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH3:7])[C:2]=1[CH3:8]

Participants

5

Reactant 4

HCID 311Citric AcidHCID 961HydroxideHCID 6328Methyl iodideHCID 114202,3-Lutidine

Product 1

HCID 131712653HCID 131712653, compound

Procedure

2-3-Lutidine is reacted with methyl iodide; the halide intermediate is converted to the hydroxide with Rexyn 201, and then reacted with citric acid.

Sources & evidence

ORD record
ord-f17d9df8e80e47b98a1ca4d97312b7d5
Source dataset
uspto-grants-1982_01
Patent number
US04312367

Reaction notes

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