HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citric Acid → HCID 131712654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citric Acid | HCID 311 | — |
| Reactant | Hydroxide | HCID 961 | — |
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | 2-Butene, 1-bromo-3-methyl- | HCID 70092 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 131712654 | HCID 131712654 | — |
Reaction Steps
3-Acetylpyridine is reacted with 1-bromo-3-methyl-2-butene in acetonitrile; the halide intermediate is converted to the hydroxide in methanolic sodium hydroxide, and then reacted with citric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04312367 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-857fe28dfbea46d582099afa4678bd44 |
| Source note | uspto-grants-1982_01 |