HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12893740, compound → HCID 12893742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12893740 | HCID 12893740 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 12893742 | HCID 12893742 | — |
Reaction Steps
10 Grams of the 9-oxodec-4-ynoic acid of Example 18 is hydrogenated at room temperature in toluene containing about 0.5% quinoline with 5% palladium on barium sulfate as catalyst. The toluene solution is washed with 1 N hydrochloric acid, then water. The solution is dried over sodium sulfate and stripped of solvent to give, as a yellow oil, the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04312994 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-f62e2eadc348493aa266a781a15b4e77 |
| Source note | uspto-grants-1982_01 |