HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Indanone → 2-[(Dimethylamino)methylene]-2,3-dihydro-1H-inden-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Indanone | HCID 6735 | — |
| Reactant | Dimethylformamide diethylacetal | HCID 70913 | — |
| Product | 2-[(Dimethylamino)methylene]-2,3-dihydro-1H-inden-1-one | HCID 99044 | — |
Reaction Steps
The 2-(dimethylaminomethylene)-indan-1-one starting material was prepared from 1-indanone (3.17 g, 24 mmol) and N,N-dimethylformamide diethyl acetal (21 ml, 120 mmol) to give the desired product as golden yellow crystals (2.61 g) m.p. 156-161°. MS (ES+) 188 (MH+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057329 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-f7dd204966e84429ace60fbe2d8e2725 |
| Source note | uspto-grants-2000_05 |