HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide diethylacetal → HCID 54306991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide diethylacetal | HCID 70913 | — |
| Reactant | 7-Methyltetralone | HCID 89147 | — |
| Product | HCID 54306991 | HCID 54306991 | — |
Reaction Steps
3,4-Dihydro-2-dimethylaminomethylene-7-methyl-1(2H) naphthalenone was prepared from 7-methyl-1-tetralone (4.8 g, 30 mmol) and N,N-dimethyl-formamide diethyl acetal (15.4 ml, 90 mmol). The crude product was recrystallised from diethyl ether-hexane to give yellow crystals (4.64 g) m.p. 79-82° MS (ES+) 238 (MNa+, 6%), 216 (MH+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057329 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-38ea26150f144d9e81f21add8440897c |
| Source note | uspto-grants-2000_05 |