Tributylphenyltin → HCID 18789336, compound
Reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([C:8]2[NH:12][N:11]=[C:10]([NH:13][C:14]([CH:16]3[CH2:24][C:23]4[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=4)[CH2:17]3)=[O:15])[CH:9]=2)=[CH:4][CH:3]=1.C(C([Sn])=[C:30]([CH2:35][CH2:36][CH2:37][CH3:38])[CH2:31]CCC)CCC.BrC1C=C(C2NN=C(NC(C3CC4C(=CC=CC=4)C3)=O)C=2)C=CC=1.C([Sn](CCCC)(CCCC)C1C=CC=CC=1)CCC>>[C:7]1([C:31]2[CH:30]=[CH:35][CH:36]=[CH:37][CH:38]=2)[CH:2]=[CH:3][CH:4]=[C:5]([C:8]2[NH:12][N:11]=[C:10]([NH:13][C:14]([CH:16]3[CH2:24][C:23]4[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=4)[CH2:17]3)=[O:15])[CH:9]=2)[CH:6]=1Participants
5
Procedure
The title compound was prepared in the same manner as that described in Example 33 except that 5-(4-bromophenyl)-3-(2-indanyl)carbonylaminopyrazole and tributylvinyltin used in Example 33 were replaced with 5-(3-bromophenyl)-3-(2-indanyl)carbonylaminopyrazole and tributylphenyltin, respectively.
Sources & evidence
- ORD record
- ord-e0f7e089f5a34911afffe0a948a96c41
- Source dataset
- uspto-grants-2000_05
- Patent number
- US06057335
Reaction notes
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