HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22675560, compound → HCID 22675476, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22675560 | HCID 22675560 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22675476 | HCID 22675476 | 104.8% |
Reaction Steps
Methyl 4-[2-(2-(2-chloro-2-(phenyl )ethyl)-3-pyridyl)ethyl]benzoate (0.537 g, 1.29mmol) was dissolved in ethanol (10 ml). The solution was treated with palladium on carbon (10% Pd, 0.1 g) and placed under a hydrogen atmosphere. The reaction was stirred at ambient temperature for 18 hours, then filtered and the solvent evaporated to give methyl 4-[2-(2-(phenethyl)-3-pyridyl)ethyl]benzoate (0.467 g), which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057345 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-5dec68b831354375981e0ce95e69593e |
| Source note | uspto-grants-2000_05 |