HRID1106933

反应详情

EQUATION

反应方程式

HRID 1106933 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of (R/S)-1-(1-adamantyl)methyl-1,2,3,4-tetrahydro-9H-pyrido[3,4-b]indole (640 mg, 2.0 mmol) and succinic anhydride (250 mg, 2.5 mmol) was stirred in dioxan (5 ml) at room temperature for 17 hours. The white precipiate which had formed was isolated by filtration, washed with dioxan and dried. (640 mg, 76%).

WORKUP

后处理

  1. customThe white precipiate which had formed
  2. customwas isolated by filtration
  3. washwashed with dioxan
  4. customdried