反应详情

Being cooled in an ice-water bath, a solution of 50.5 ml of butyl lithium(0.126 mol) in 2.5M hexane were slowly dripped to a solution of 15.4 g(0.126 mol) of butyl-cyclopentadiene(manufactured by RIPP) in 100 ml THF with stirring. After the dripping was finished, the resultant mixture was continuously stirred for 1 hour, a white muddy solution of butyl-cyclopentadienyl lithium was obtained.

1. temperatureBeing cooled in an ice-water bath