HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 86755400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 86755399 | HCID 86755399 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 86755400 | HCID 86755400 | — |
Reaction Steps
15.20 g (19.56 mmol) 20 was taken up in 200 ml CH2Cl2 /TFA (3:1 v/v) and stirred for 30 min. Afterwards the solution was diluted with 200 ml CH2Cl2 and shaken out with 200 ml sat. NaHCO3 solution. The organic phase was dried over MgSO4 and rotary evaporated. Yield: 11.64 g (88%) 21 as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060455 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-636d1c79b88d417e9ea6de1918e0d924 |
| Source note | uspto-grants-2000_05 |