HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 135670758, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 135670800 | HCID 135670800 | — |
| Product | HCID 135670758 | HCID 135670758 | — |
Reaction Steps
In a similar manner to Example 78, 3-methylthio-8-oxo-6-(2-propoxyphenyl)-7,8-dihydropyrimido[4,5-e][1,2,4]triazine (0.5 g) was treated for 3 hours with sodium methoxide (prepared from sodium, 0.17 g, and methanol) to afford the title compound, 0.34 g, m.p. 234-235° C. (recrystallized from methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060477 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-f7297c0947714cb3bc2cce96d6a7cccd |
| Source note | uspto-grants-2000_05 |