HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl benzofuran-7-carboxylate → Methyl 2,3-dihydrobenzofuran-7-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl benzofuran-7-carboxylate | HCID 14229730 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Methyl 2,3-dihydrobenzofuran-7-carboxylate | HCID 15062252 | 100% |
Reaction Steps
Methyl benzofuran-7-carboxylate (12 g, 68 mmol) was hydrogenated at 60 psi over 10% Pd/C (2 g) in acetic acid (60 ml) for 18 hr. The mixture was filtered, and the filtrate was concentrated in vacuo to give a pale green oil (12 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060506 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-3dffc0c706454937a2821782022a9319 |
| Source note | uspto-grants-2000_05 |