HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydro-2,2-dimethyl-4-benzofurancarboxylic acid → HCID 18787456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydro-2,2-dimethyl-4-benzofurancarboxylic acid | HCID 14838233 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 18787456 | HCID 18787456 | 93% |
Reaction Steps
2,2-Dimethyl-2,3-dihydro-benzofuran-4-carboxylic acid (8.6 g, 45 mmol) was reduced with LAH (3.41 g, 89 mmol) similar to the above procedures to give the product as a clear oil (7.35 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060506 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-05677e5fbd3341508d2543f9cb652795 |
| Source note | uspto-grants-2000_05 |