Ethanethiol → HCID 9850075, compound

Participants

Reaction Steps

6-Methoxy-2-(4-methoxyphenyl)-3-(4-[1-benzylpiperidin-4-oxy]benzoyl)benzo[b]thiophene (846 mg, 1.50 mmol), ethane thiol (7.50 mmol), and aluminum chloride (1.2 g, 9.00 mmol) were converted to 450 mg (56%) of the title compound by the procedure of Example 16. MS(FD) 536(M+). IR (CHCl3) ν max 3311, 3023, 3011, 2953, 1721, 1596, 1469, 1257, 1166.

Provenance & Evidence