Benzyl Alcohol → HCID 15888171, compound

HRID 1107738Notes

Reaction equation

HRID 1107738 reaction equation
Cl[C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]3[CH2:16][CH2:15]3)[C:7]=12.[CH2:17]([OH:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[CH2:17]([O:24][C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]3[CH2:16][CH2:15]3)[C:7]=12)[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 244Benzyl AlcoholHCID 18785706HCID 18785706, compound

Product 1

HCID 15888171HCID 15888171, compoundYield 69.2%

Procedure

The title compound was prepared as a white powder in 69.2% yield in a similar procedure to that described in Example 1 by using 7-chloro-1-cyclopropylmethyl-2,3-dimethylpyrrolo[2,3-d]pyridazine and benzyl alcohol.

Sources & evidence

ORD record
ord-e9bda606ba6b473c8e2b763d34f9f1ff
Source dataset
uspto-grants-2000_05
Patent number
US06063782

Reaction notes

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