Benzyl Alcohol → HCID 54388272, compound

HRID 1107740Notes

Reaction equation

HRID 1107740 reaction equation
Cl[C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]=[CH:15][C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)[C:7]=12.[CH2:22]([OH:29])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[CH2:22]([O:29][C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]=[CH:15][C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)[C:7]=12)[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 244Benzyl AlcoholHCID 54156760HCID 54156760, compound

Product 1

HCID 54388272HCID 54388272, compoundYield 85.4%

Procedure

The title compound (trans) was prepared as pale brown crystals in 85.4% yield in a similar procedure to that described in Example 1 by using 7-chloro-2,3-dimethyl-1-(3-phenyl-2-propenyl)pyrrolo[2,3-d]pyridazine (trans) and benzyl alcohol.

Sources & evidence

ORD record
ord-ffac8b43cad74cb78537cadfb97b90d6
Source dataset
uspto-grants-2000_05
Patent number
US06063782

Reaction notes

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