Benzyl Alcohol → HCID 53849954, compound

HRID 1107744Notes

Reaction equation

HRID 1107744 reaction equation
Cl[C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]=[CH:15][CH2:16][CH3:17])[C:7]=12.[CH2:18]([OH:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH2:18]([O:25][C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]=[CH:15][CH2:16][CH3:17])[C:7]=12)[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

3

Reactant 2

HCID 244Benzyl AlcoholHCID 54512843HCID 54512843, compound

Product 1

HCID 53849954HCID 53849954, compoundYield 75.9%

Procedure

The title compound (trans) was prepared as a white powder in 75.9% yield in a similar procedure to that described in Example 1 by using 7-chloro-2,3-dimethyl-1-(2-pentenyl)pyrrolo[2,3-d]pyridazine (trans) and benzyl alcohol.

Sources & evidence

ORD record
ord-cd9aff0a9bd244578000df4a9f4d80e7
Source dataset
uspto-grants-2000_05
Patent number
US06063782

Reaction notes

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