HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinemethanol → 1-(2-Butenyl)-2,3-dimethyl-7-(3-pyridylmethyloxy)pyrrolo[2,3-d]pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinemethanol | HCID 7510 | — |
| Reactant | 1-(2-Butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53719624 | — |
| Product | 1-(2-Butenyl)-2,3-dimethyl-7-(3-pyridylmethyloxy)pyrrolo[2,3-d]pyridazine | HCID 54274703 | 45.9% |
Reaction Steps
The title compound (cis/trans=22/78) was prepared as a pale yellow powder in 45.9% yield in a similar procedure to that described in Example 1 by using 1-(2-butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine (cis/trans=20/80) and 3-pyridinemethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06063782 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-c77aeee2fd294e5ca0504fb5d230a2c9 |
| Source note | uspto-grants-2000_05 |