Furfuryl Alcohol → HCID 54323414, compound

HRID 1107764Notes

Reaction equation

[CH2:1]([N:5]1[C:9]2=[C:10](Cl)[N:11]=[N:12][CH:13]=[C:8]2[C:7]([CH3:15])=[C:6]1[CH3:16])[CH:2]=[CH:3][CH3:4].[CH2:17]([OH:23])[C:18]1[O:22][CH:21]=[CH:20][CH:19]=1>>[CH2:1]([N:5]1[C:9]2=[C:10]([O:23][CH2:17][C:18]3[O:22][CH:21]=[CH:20][CH:19]=3)[N:11]=[N:12][CH:13]=[C:8]2[C:7]([CH3:15])=[C:6]1[CH3:16])[CH:2]=[CH:3][CH3:4]

Participants

Reactant 2

HCID 7361Furfuryl Alcohol

HCID 537196241-(2-Butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine

Product 1

HCID 54323414HCID 54323414, compoundYield 12.2%

Procedure

The title compound (cis/trans=15/85) was prepared as a flesh-colored powder in 12.2% yield in a similar procedure to that described in Example 1 by using 1-(2-butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine (cis/trans=20/80) and furfuryl alcohol.

Sources & evidence

ORD record: ord-e07cf519bcff4749870da74f6f793678
Source dataset: uspto-grants-2000_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06063782

Reaction notes

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