Benzylamine → HCID 54055664, compound

HRID 1107774Notes

Reaction equation

HRID 1107774 reaction equation
Cl[C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]=[CH2:15])[C:7]=12.[CH2:16]([NH2:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH2:16]([NH:23][C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH:13]=[CH:14][CH3:15])[C:7]=12)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 18785586HCID 18785586, compound

Product 1

HCID 54055664HCID 54055664, compoundYield 31.5%

Procedure

The title compound (trans) was prepared as a beige powder in 31.5% yield in a similar procedure to that described in Example 44 by using 7-chloro-2,3-dimethyl-1-(2-propenyl)pyrrolo[2,3-d]pyridazine and benzylamine.

Sources & evidence

ORD record
ord-d4c47bd30a9e4458b5e0f8157c82ae3c
Source dataset
uspto-grants-2000_05
Patent number
US06063782

Reaction notes

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