4-Chlorobenzyl mercaptan → HCID 54227206, compound

HRID 1107783Notes

Reaction equation

HRID 1107783 reaction equation
Cl[C:2]1[N:3]=[N:4][CH:5]=[C:6]2[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]=[CH2:15])[C:7]=12.[Cl:16][C:17]1[CH:22]=[CH:21][C:20]([CH2:23][SH:24])=[CH:19][CH:18]=1>>[Cl:16][C:17]1[CH:22]=[CH:21][C:20]([CH2:23][S:24][C:2]2[N:3]=[N:4][CH:5]=[C:6]3[C:10]([CH3:11])=[C:9]([CH3:12])[N:8]([CH2:13][CH:14]=[CH2:15])[C:7]=23)=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 804094-Chlorobenzyl mercaptanHCID 18785586HCID 18785586, compound

Product 1

HCID 54227206HCID 54227206, compoundYield 70.6%

Procedure

The title compound was prepared as a yellow solid in 70.6% yield in a similar procedure to that described in Example 1 by using 7-chloro-2,3-dimethyl-1-(2-propenyl)pyrrolo[2,3-d]pyridazine and 4-chlorophenylmethanethiol.

Sources & evidence

ORD record
ord-54091f3edb1c45c3bc736beae9eef178
Source dataset
uspto-grants-2000_05
Patent number
US06063782

Reaction notes

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