7-Benzyloxy-2,3-dimethylpyrrolo[2,3-d]pyridazine → HCID 54222496, compound

HRID 1107788Notes

Reaction equation

HRID 1107788 reaction equation
[CH2:1]([O:8][C:9]1[N:10]=[N:11][CH:12]=[C:13]2[C:17]([CH3:18])=[C:16]([CH3:19])[NH:15][C:14]=12)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.CS(O[CH2:25][CH:26]=[CH:27][C:28]([F:31])([F:30])[F:29])(=O)=O>>[CH2:1]([O:8][C:9]1[N:10]=[N:11][CH:12]=[C:13]2[C:17]([CH3:18])=[C:16]([CH3:19])[N:15]([CH2:25][CH:26]=[CH:27][C:28]([F:31])([F:30])[F:29])[C:14]=12)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 187856837-Benzyloxy-2,3-dimethylpyrrolo[2,3-d]pyridazineHCID 53958317HCID 53958317, compound

Product 1

HCID 54222496HCID 54222496, compoundYield 20.7%

Procedure

The title compound was prepared as pale yellow crystals in 20.7% yield in a similar procedure to that described in Example 41-by using 7-benzyloxy-2,3-dimethylpyrrolo[2,3-d]pyridazine and 4,4,4-trifluoro-2-butenyl methanesulfonate.

Sources & evidence

ORD record
ord-f9def2dbf82c4d9eaae80460f50c2192
Source dataset
uspto-grants-2000_05
Patent number
US06063782

Reaction notes

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