2-Bromo-1,1-difluoroethane → HCID 18785656, compound

HRID 1107802Notes

Reaction equation

HRID 1107802 reaction equation
[CH:1]([C:3]1[C:7]([CH3:8])=[C:6]([CH3:9])[NH:5][C:4]=1[C:10]([O:12][CH3:13])=[O:11])=[O:2].Br[CH2:15][CH:16]([F:18])[F:17]>>[F:17][CH:16]([F:18])[CH2:15][N:5]1[C:6]([CH3:9])=[C:7]([CH3:8])[C:3]([CH:1]=[O:2])=[C:4]1[C:10]([O:12][CH3:13])=[O:11]

Participants

3

Reactant 2

HCID 1361862-Bromo-1,1-difluoroethaneHCID 10773740Methyl 3-formyl-4,5-dimethyl-1H-pyrrole-2-carboxylate

Product 1

HCID 18785656HCID 18785656, compound

Procedure

The title compound was prepared as flesh-colored crystals in 90.4% yeild in a similar procedure to that described in Referential Example 9 by using methyl 3-formyl-4,5-dimethylpyrrole-2-carboxylate and 2-bromo-1,1-difluoroethane.

Sources & evidence

ORD record
ord-5fa056c0d50a462ea2796544ca3d43e6
Source dataset
uspto-grants-2000_05
Patent number
US06063782

Reaction notes

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