Methyl 3-formyl-4,5-dimethyl-1H-pyrrole-2-carboxylate → HCID 54460326, compound
Reaction equation
[CH:1]([C:3]1[C:7]([CH3:8])=[C:6]([CH3:9])[NH:5][C:4]=1[C:10]([O:12][CH3:13])=[O:11])=[O:2].CS(O[CH2:19][CH:20]=[CH:21][C:22]([F:25])([F:24])[F:23])(=O)=O>>[CH:1]([C:3]1[C:7]([CH3:8])=[C:6]([CH3:9])[N:5]([CH2:19][CH:20]=[CH:21][C:22]([F:25])([F:24])[F:23])[C:4]=1[C:10]([O:12][CH3:13])=[O:11])=[O:2]Participants
3
Procedure
The title compound (trans) was prepared as a pale yellow oil in 60.0% yeild in a similar procedure to that described in Referential Example 9 by using methyl 3-formyl-4,5-dimethylpyrrole-2-carboxylate and 4,4,4-trifluoro-2-butenyl methanesulfonate (trans).
Sources & evidence
- ORD record
- ord-ceafdd1a56b24ccaa770d6fc2cce229d
- Source dataset
- uspto-grants-2000_05
- Patent number
- US06063782
Reaction notes
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