HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → 3-Butenylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-Butenylbenzene | HCID 13033 | 94% |
Reaction Steps
Example 1 was repeated except that 1.0 L of tetrahydrofuran was used as a solvent in place of the mixed solvent of 250 ml of tetrahydrofuran and 750 ml of toluene, and 127.0 g (yield 94%) of 4-phenyl-1-butene was obtained. The analysis of the product by gas chromatography indicated the purity of 98.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06063940 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-96b318ca8da44a1696b1a09242f5fcea |
| Source note | uspto-grants-2000_05 |