HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → Benzyl 2,3-dihydrofuran-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 3-Furoic acid | HCID 10268 | — |
| Product | Benzyl 2,3-dihydrofuran-3-carboxylate | HCID 18785169 | — |
Reaction Steps
Synthesis takes place first of all by Birch reduction of 3-furancarboxylic acid followed by esterification with benzyl bromide to form benzyl 2,3-dihydrofuran-3-carboxylate (in accordance with G. Lowe, St. Swain; J. Chem. Soc. Perkin Trans I (1985), 391) ##STR29## b) The end product from a) is reduced with lithium aluminum hydride to give 3-hydroxymethyl-2,3-dihydrofuran
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06066746 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-0b3b7cc51dd74bfab1171537632f93c7 |
| Source note | uspto-grants-2000_05 |