HCID 54028665, compound → HCID 22627191, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of methyl 3-(2-methoxycarbonylethenyl)indole-6-carboxylate (213 mg) in a mixture of 1,4-dioxane (2 ml) and methanol (3 ml) was added 10% palladium on carbon (40 mg) and the mixture was stirred under hydrogen at 20° C. for 6.5 hours. The resulting mixture was filtered through celite and the filtrate was evaporated in vacuo. The residue was triturated with diisopropyl ether to give methyl 3-(2-methoxycarbonylethyl)indole-6-carboxylate (177 mg).

Provenance & Evidence