HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Iodothiophene → 3-(2-Thienyl)propiolamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Iodothiophene | HCID 18921 | — |
| Reactant | Propynamide | HCID 101445 | — |
| Product | 3-(2-Thienyl)propiolamide | HCID 18784294 | 55% |
Reaction Steps
According to preparation 4, propiolamide (1.68 g, 24.45 mmol) was coupled with 2-iodothiophene (3.2 g, 15.67 mmol) to provide 1.29 g (55%) of product. NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06069247 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-0d11549e47e54fd69bb0c2c35d5ed29b |
| Source note | uspto-grants-2000_05 |