Hydrazine → N-(2,2,6,6-tetramethyl-4-piperidinyl)-N'-aminosuccinamide

HRID 1108939Notes

Reaction equation

HRID 1108939 reaction equation
[NH2:1][CH:2]1[CH2:7][C:6]([CH3:9])([CH3:8])[NH:5][C:4]([CH3:11])([CH3:10])[CH2:3]1.C([CH:14]([CH2:18][C:19](Cl)=[O:20])[C:15](Cl)=[O:16])C.[NH2:22][NH2:23]>CO>[CH3:8][C:6]1([CH3:9])[CH2:7][CH:2]([NH:1][C:15](=[O:16])[CH2:14][CH2:18][C:19]([NH:22][NH2:23])=[O:20])[CH2:3][C:4]([CH3:11])([CH3:10])[NH:5]1

Participants

5

Reactant 3

HCID 9321HydrazineHCID 375244-Amino-2,2,6,6-tetramethylpiperidineHCID 218646082-Ethylbutanedioyl dichloride

Product 1

HCID 14745323N-(2,2,6,6-tetramethyl-4-piperidinyl)-N'-aminosuccinamide

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

N-(2,2,6,6-tetramethyl-4-piperidinyl)-N'-aminosuccinamide was prepared by the reaction of 4-amino-2,2,6,6-tetramethylpiperidine with ethyl succinyl chloride followed by hydrazinolysis of the resulting ester with 64% aqueous hydrazine in methanol.

Sources & evidence

ORD record
ord-36574f3f395447b39bf10ee89306327b
Source dataset
uspto-grants-1994_06
Patent number
US05318851

Reaction notes

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