6639-66-3 → HCID 15227802, compound

HRID 1108986Notes

Reaction equation

HRID 1108986 reaction equation
[CH3:1][O:2][C:3]1[C:11]([O:12][CH3:13])=[C:10]([O:14][CH3:15])[CH:9]=[C:8]2[C:4]=1[CH2:5][CH2:6][C:7]2=O.CC1C=CC(N=[CH:25][C:26]2[C:27]([NH2:35])=[CH:28][C:29]3[O:33][CH2:32][O:31][C:30]=3[CH:34]=2)=CC=1>>[CH3:15][O:14][C:10]1[C:11]([O:12][CH3:13])=[C:3]([O:2][CH3:1])[C:4]2[CH2:5][C:6]3[C:7]([C:8]=2[CH:9]=1)=[N:35][C:27]1[CH:28]=[C:29]2[O:33][CH2:32][O:31][C:30]2=[CH:34][C:26]=1[CH:25]=3

Participants

3

Reactant 2

HCID 2416176639-66-3HCID 190217004,5,6-Trimethoxy-2,3-dihydro-1H-inden-1-one

Product 1

HCID 15227802HCID 15227802, compoundYield 49.9%

Procedure

Using the procedure of Example 1, 4,5,6-trimethoxyindan-1-one (1.10 mg, 4.8 mmol) is reacted with 6[[(4-methylphenyl)imino]methyl]-1,3-benzodioxol-5-amine (1.22 g, 4.8 mmol) to yields 7,8,9-trimethoxy-10H-1,3-dioxolo[4,5-g]indeno[1,2-b]quinoline (0.84 mg, 49.9% of theory).

Sources & evidence

ORD record
ord-11d88cd43bb1453583a21bd9d3552364
Source dataset
uspto-grants-1994_06
Patent number
US05318976

Reaction notes

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