5,6-Dimethoxy-1-indanone → HCID 15227801, compound

HRID 1108987Notes

Reaction equation

HRID 1108987 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][C:11]=1[O:12][CH3:13])[C:8](=O)[CH2:7][CH2:6]2.CC1C=CC(N=[CH:23][C:24]2[C:25]([NH2:33])=[CH:26][C:27]3[O:31][CH2:30][O:29][C:28]=3[CH:32]=2)=CC=1>>[CH3:13][O:12][C:11]1[C:3]([O:2][CH3:1])=[CH:4][C:5]2[CH2:6][C:7]3[C:8]([C:9]=2[CH:10]=1)=[N:33][C:25]1[CH:26]=[C:27]2[O:31][CH2:30][O:29][C:28]2=[CH:32][C:24]=1[CH:23]=3

Participants

3

Reactant 2

HCID 750185,6-Dimethoxy-1-indanoneHCID 2416176639-66-3

Product 1

HCID 15227801HCID 15227801, compoundYield 81%

Procedure

Using the procedure of Example 1, 5,6-dimethoxyindan-1-one (192 mg, 1 mmol) is reacted with 6[[(4-methylphenyl)imino]methyl]-1,3-benzodioxol-5-amine (255 mg, 1 mmol) to yields 7,8-dimethoxy-10H-1,3-dioxolo[4,5-g]indeno[1,2-b]quinoline (260 mg, 81 % of theory).

Sources & evidence

ORD record
ord-d17e3eca03af4a638db3bd4bd40c9e7c
Source dataset
uspto-grants-1994_06
Patent number
US05318976

Reaction notes

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