6639-66-3 → HCID 15227803, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6]([CH2:7][CH2:8][C:9]2=O)=[CH:5][CH:4]=1.CC1C=CC(N=[CH:21][C:22]2[C:23]([NH2:31])=[CH:24][C:25]3[O:29][CH2:28][O:27][C:26]=3[CH:30]=2)=CC=1>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[CH2:7][C:8]3[C:9]([C:10]=2[CH:11]=1)=[N:31][C:23]1[CH:24]=[C:25]2[O:29][CH2:28][O:27][C:26]2=[CH:30][C:22]=1[CH:21]=3Participants
3
Procedure
Using the procedure of Example 1, 6-methoxyindan-1-one (162 mg, 1 mmol) is reacted with 6[[(4-methylphenyl)imino]methyl]-1,3-benzodioxol-5-amine (255 mg, 1 mmol) to yields 7-methoxy-10H-1,3-dioxolo[4,5-g]indeno[1,2-b]quinoline (130 mg, 44.6% of theory).
Sources & evidence
- ORD record
- ord-15c92a2a75ca4a319b1857fd7019b84f
- Source dataset
- uspto-grants-1994_06
- Patent number
- US05318976
Reaction notes
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