6639-66-3 → HCID 19021698, compound

HRID 1108994Notes

Reaction equation

HRID 1108994 reaction equation
[CH3:1][O:2][CH2:3][O:4][C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][C:13]=1[O:14][CH2:15][O:16][CH3:17])[C:10](=O)[CH2:9][CH2:8]2.CC1C=CC(N=[CH:27][C:28]2[C:29]([NH2:37])=[CH:30][C:31]3[O:35][CH2:34][O:33][C:32]=3[CH:36]=2)=CC=1>>[CH3:17][O:16][CH2:15][O:14][C:13]1[C:5]([O:4][CH2:3][O:2][CH3:1])=[CH:6][C:7]2[CH2:8][C:9]3[C:10]([C:11]=2[CH:12]=1)=[N:37][C:29]1[CH:30]=[C:31]2[O:35][CH2:34][O:33][C:32]2=[CH:36][C:28]=1[CH:27]=3

Participants

3

Reactant 2

HCID 2416176639-66-3HCID 19021692HCID 19021692, compound

Product 1

HCID 19021698HCID 19021698, compoundYield 40.2%

Procedure

Using the procedure of Example 1, 5,6-dimethoxymethoxyindan-1-one (504 mg, 2 mmol) is reacted with 6[[(4-methylphenyl)imino]methyl]-1,3-benzodioxol-5-amine (508 mg, 2 mmol) to yields 7,8-dimethoxymethoxy-10H-1,3-dioxolo[4,5-g]indeno[1,2-b]quinoline (307 mg, 40% of theory).

Sources & evidence

ORD record
ord-13e50db943f54bfeac719d42db1fa74f
Source dataset
uspto-grants-1994_06
Patent number
US05318976

Reaction notes

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