6639-66-3 → HCID 19021690, compound

HRID 1108995Notes

Reaction equation

HRID 1108995 reaction equation
[CH3:1][O:2][CH2:3][O:4][C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[C:10](=O)[CH2:9][CH2:8]2.CC1C=CC(N=[CH:23][C:24]2[C:25]([NH2:33])=[CH:26][C:27]3[O:31][CH2:30][O:29][C:28]=3[CH:32]=2)=CC=1>>[CH3:1][O:2][CH2:3][O:4][C:5]1[CH:13]=[CH:12][C:11]2[C:10]3=[N:33][C:25]4[CH:26]=[C:27]5[O:31][CH2:30][O:29][C:28]5=[CH:32][C:24]=4[CH:23]=[C:9]3[CH2:8][C:7]=2[CH:6]=1

Participants

3

Reactant 2

HCID 2416176639-66-3HCID 19021688HCID 19021688, compound

Product 1

HCID 19021690HCID 19021690, compoundYield 15.8%

Procedure

Using the procedure of Example 1, 5-methoxymethoxyindan-1-one (327 mg, 1.7 mmol) is reacted with 6[[(4-methylphenyl)imino]methyl]-1,3-benzodioxol-5-amine (432 mg, 1.7 mmol) to yields 8-methoxymethoxy-10H-1,3-dioxolo[4,5-g]indeno[1,2-b]quinoline (86.3 mg, 15% of theory).

Sources & evidence

ORD record
ord-fa49b8b67a2b4279bd8d5192806af2e7
Source dataset
uspto-grants-1994_06
Patent number
US05318976

Reaction notes

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